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Where equilibrium concentration of adsorbed Cu (II) ions is taken as qe (mmol g-1) and the same at time t (min) is represented as qt (mmol g-1), respectively and pseudo-first order rate constant as k1 (min-1).
Initial sorption rate ho (mmol g-1 min-1) was determined from the value of rate constant (k2) using Eq.
1-Bromo-3-phenylpropane (7c) (72 pl, 0.47 mmol), Na[N.sub.3] (40.66 mg, 0.63 mmol), 6 (100.18 mg, 0.46 mmol), CuS[O.sub.4]-5[H.sub.2]O (60.94 mg, 0.24 mmol), and sodium ascorbate (10.66 mg, 0.054 mmol).
p-(2-Bromoethyl)toluene (9a) (157.18 [micro]l, 1.03 mmol), Na[N.sub.3] (75.92 mg, 1.16 mmol), 6 (154.02 mg, 0.71 mmol), CuS[O.sub.4] x 5[H.sub.2]O (38.42 mg, 0.15 mmol), and sodium ascorbate (15.49 mg, 0.08 mmol).
In another experiment, the hippocampus was perfused with ACSF for 25 min to determine the basal concentrations of glutamate in the extracellular fluid; then perfused with 1 mmol [1.sup.-1] DHMBA in ACSF or 10 [micro]mol [1.sup.-1] Zn[Cl.sub.2] in ACSF for 25 min; and, finally, perfused with 1 mmol [1.sup.-1] DHMBA in ACSF containing 100 mmol [1.sup.-1] KCl or 10 [micro]mol [1.sup.-1] Zn[Cl.sub.2] in ACSF containing 100 mmol [1.sup.-1] KCl, respectively, for 5 min.
n-Butyllithium 1.6 mol/L (8.60 mL, 13.7 mmol) was added to a solution of compound 9 (2.00 g, 6.87 mmol) in anhydrous tetrahydrofuran (35 mL) under nitrogen atmosphere at -78 [degrees]C, which was followed by addition of dimethylformamide (1.00 g, 13.7 mmol, 1.06 mL).
The desired average rate of total Ca increase expressed in mmol [L.sup.-1] [min.sup.-1] is defined as the amount of Ca (in mmol) that was added in the total volume of reactant solution (in L) after 1 -min titration.
After taxi drivers estate agents had the highest cholesterol levels at 5.5 mmol.
There was also no significant difference in total natriuresis calculated according to the excreted volume (empagliflozin 83.3 mmol ([+ or -] 42) versus placebo 64.4 mmol ([+ or -] 41); treatment effect 8.54mmol/l (CI -14.19, 31.27), p = 0.5) however with an increase in the empagliflozin group towards the end of the observation period (Figure 2).
Acid chlorides (2a-2p) required in the preparation of gamma keto esters (3a-3p) were prepared by the reaction of di-/tri-substitutedbenzyl hydrogen succinates (8 mmol)) and thionyl chloride (22.5 mmol).
(11) This concept was hypothetically supported in case 2, in which there was a clear diagnosis of SIADH (as demonstrated with an initial urine [Na.sup.+] level of 189 mmol/l and urine osmolality of 788 mOsmol/kg [H.sub.2]O) associated with only a modest rise in blood [Na.sup.+] (11 mmol/l) with administration of 1.3 litres of 5% saline (1 113 mmol [Na.sup.+] total).
The rapid overcorrection of sodium (10 mmol/L in the first 12 h) increased the risk of osmotic demyelination because complications have been noted if the serum sodium change is >0.55 mmol x [L.sup.-1] x [h.sup.-1] (>10 mmol/L in 24 h and >18 mmol/L in 48 h).
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